International Journal of Advanced Materials Research
Articles Information
International Journal of Advanced Materials Research, Vol.5, No.1, Mar. 2019, Pub. Date: May 5, 2019
Phase Transformation Kinetics and Microstructure Evolution in a Medium Carbon Nano-structured Bainitic Steel During Isothermal Annealing Treatment
Pages: 12-19 Views: 1313 Downloads: 359
Authors
[01] Sanjeev Kumar Shukla, R&D Centre for Iron & Steel (RDCIS), Steel Athority of India Ltd. (SAIL), Ranchi, India.
[02] Mohammad Serfraj Alam, R&D Centre for Iron & Steel (RDCIS), Steel Athority of India Ltd. (SAIL), Ranchi, India.
[03] Kartik Nageswaran, R&D Centre for Iron & Steel (RDCIS), Steel Athority of India Ltd. (SAIL), Ranchi, India.
[04] Vinod Kumar, R&D Centre for Iron & Steel (RDCIS), Steel Athority of India Ltd. (SAIL), Ranchi, India.
[05] Santosh Kumar, R&D Centre for Iron & Steel (RDCIS), Steel Athority of India Ltd. (SAIL), Ranchi, India.
Abstract
To examine the influence of isothermal annealing treatment both below and above Ms temperature on the transformation kinetics and microstructure evolution in a medium carbon nano-structured bainitic steel, dilatometry studies were conducted in a Thermo-mechanical simulator (Gleeble-3500 C) in a steel of compostion C: 0.49%, Mn: 1.46%, S: 0.019%, P: 0.003%, Si: 1.78%, Cr: 1.12% & Mo: 0.17% having Ms temperature ~270°C. The heat treatment cycle comprised of heating the samples at 5°C/s to austenitizing temperature of 850°C, soaking at 850°C for 180 seconds, cooling at 20°C/s upto the isothermal annealing temperature varying from 180°C to 360°C, holding at these temperatures for 8 hrs. followed by natural cooling upto room temperature. Microstructure at and above Ms temperature comprised lower bainite (accompanied by carbide precipitation) alongwith retained austenite and martensite-austenite (MA) blocks, while below Ms temperature, besides tempered martensite, features of typical lower bainite were observed alongwith carbides aligned in ferrite platelets. Phase transformation kinetics was analysed through dilatometry plots. It has been found that formation of prior athermal martensite causes an acceleration at the start of the subsequent isothermal transformations below Ms temperature compared to those above Ms temperature, where prior martensite does not form, which is reflected in high incubation time for bainitic transformation in such cases.
Keywords
Nano-structured Bainitic Steel, Phase Transformation Kinetics, Thermo-mechanical Simulation
References
[01] Bhadeshia H. K. D. H., “Bainite in steels: transformations, microstructure and properties”, 2nd edition, London: IOM Communications, 2001, pp. 735.
[02] Y. K. Lee, “Empirical formula of isothermal bainite start temperature of steels”, “Journal of Materials Science Letters, 21, 2002, pp. 1253-1255.
[03] E. P. Da Silva, et al., “Isothermal transformations in advanced high strength steels below martensite start temperature”, Materials Science and Technology, 2015, Vol 31. No. 7, pp..808-816.
[04] Navarro-Lo´ Pez, et al., “Effect of Prior Athermal Martensite on the Isothermal Transformation Kinetics Below Ms in a Low-C High-Si Steel”, Metallurgical and Materials Transactions A, 2015, 47 (3). pp. 1028-1039.
[05] Mohamed Soliman et al, “Development of the low temperature bainite”, Archives of Civil and Mechanical Engineering, Vol. 16, Issue 3, 2016, pp. 403-412.
[06] Junyu Tian et al., “Refined Bainite Microstructure and Mechanical Properties of a High-Strength Low-Carbon Bainitic Steel Treated by Austempering Below and Above MS”, Steel Research International, 2018, 1700469, pp. 1-10.
[07] P. Zhou et al., “Effect of Pre-Existing Martensite on Bainitic Transformation in Low-Temperature Bainite Steel”, Materials Science Forum, 2017, Vol. 898, pp. 803-809.
[08] Santigopal Samantaa et al., “Formation of bainite below the MS temperature: Kinetics and crystallography”, Acta Materialia, 2016, Vol. 105, pp. 390-403.
[09] Hamid Mousalou et al., “Microstructural and mechanical properties of low-carbon ultra-fine bainitic steel produced by multi-step austempering process”, Materials Science and Engineering A, 2018, 734, pp. 329-337.
[10] S. M. C van Bohemen et al., “Experimental evidence for bainite formation below Ms in Fe–0.66C”, Scripta Materialia, 2008, 58, pp. 488-491.
[11] M. J. Santofimia et al., “Combining bainite and martensite in steel microstructures for light weight applications”, The Journal of The Southern African Institute of Mining and Metallurgy, 2013, Vol. 113, pp. 143-148.
[12] C. Y. Wang et al., “Characterization of microstructure obtained by quenching and partitioning process in low alloy martensitic steel”, Materials Science and Engg-. A, 2010, A527, pp. 3442-3449.
[13] M. J. Santofimia et al., “Microstructural analysis of martensite constituents in quenching and partitioning steel”, Materials Characterization, Volume 92, Pages 91-95, 2014, 92, pp. 91-95.
[14] A. J. Clarke et al., “Influence of Carbon Partitioning Kinetics on Final Austenite Fraction During Quenching and Partitioning”, Scr. Mater., 2009, 61, pp. 149-152.
[15] J. Sun et al., “Study of microstructural evolution, microstructure-mechanical properties correlation and collaborative deformation-transformation behavior of quenching and partitioning (Q&P) steel”, Mater. Sci. Eng. A, 2014, 596, pp. 89-97.
600 ATLANTIC AVE, BOSTON,
MA 02210, USA
+001-6179630233
AIS is an academia-oriented and non-commercial institute aiming at providing users with a way to quickly and easily get the academic and scientific information.
Copyright © 2014 - American Institute of Science except certain content provided by third parties.